Study on bioactivity of SLMed variable gradient TC4 biomedical porous scaffolds with micro-arc oxidation treatment

Abstract

Purpose

The purpose of this paper is to improve the bioactivity of variable gradient TC4 porous scaffolds prepared by selective laser melting (SLM) through the micro-arc oxidation (MAO) technique.

Design/methodology/approach

Variable gradient TC4 porous scaffolds were prepared by SLM, then treated with MAO at different oxidation voltages. The microstructure, thickness and composition of MAO coatings were characterized by scanning electron microscope (SEM), energy-dispersive spectroscopy (EDS) and X-ray diffraction. The bioactivity of the MAO coatings was tested by simulated body fluid (SBF) immersion test.

Findings

SEM and EDS results show that with the increase of oxidation voltage, the content of Ca and P elements and the thickness of the MAO coatings increases. The thickness of the coating inside the scaffold is smaller than that of the outside regions. SBF immersion experiments showed that MAO-treated TC4 porous scaffolds had highest bioactivity at 440 V.

Originality/value

The variable gradient porous scaffolds were treated with MAO in the electrolyte containing Ca and P elements for the first time. The effect of oxidation voltages on the different region of porous scaffolds was studied in detail.

Citation

Lv, Y., Guo, J., Huang, W., Liu, Y., Liu, W. and Wei, G. (2022), "Study on bioactivity of SLMed variable gradient TC4 biomedical porous scaffolds with micro-arc oxidation treatment", Anti-Corrosion Methods and Materials, Vol. 69 No. 6, pp. 660-666. https://doi.org/10.1108/ACMM-08-2022-2684